The corrosion inhibition power of an eco-friendly green inhibitor Ixora coccinea extract (ICE) for mild steel in 1 M HCl and 0.5 M H2SO₄ was analysed using physicochemical and electrochemical techniques. 1–5 v/v% ICE was prepared and added into the corrosive acidic media for different analyses. Weight loss measurements conducted for a period of 24hrs for mild steel immersion revealed 89.38% and 77.96% inhibition capacity of ICE in 1 M HCl and 0.5 M H2SO₄ medium respectively. Electrochemical impedance parameters show that as concentration is increased, efficiency increases and double layer capacitance decreases. Potentiodynamic polarization techniques are also in good agreement with impedance studies and exhibit the mixed type inhibition character of ICE. Electrochemical noise spectrum also strongly supports the anti-corrosive property of ICE and the magnitude of noise signal decreases concerning the increase in ICE concentration. Ixorene, which is one of the major constituents of Ixora coccinea leaves was also studied for its corrosion inhibition nature by quantum mechanical calculations and was found to match with all other results. Adsorption studies of ICE are in accordance with Langmuir isotherm. Surface morphological studies confirm the formation of a protective barrier on mild steel surface in both media, i.e., 1 M HCl and 0.5 M H2SO₄.

The corrosion inhibition efficiency of the Schiff base N,N’-(5,5-dimethylcyclohexane-1,3-diylidene)dianiline (DmChDa) on mild steel in 1M HCl and 0.5M H₂SO₄ was evaluated using gravimetric, electrochemical impedance spectroscopy, potentiodynamic polarization and electrochemical noise measurement. Experimental results established that DmChDa possess relatively high corrosion inhibition capacity. Langmuir and El-Awady adsorption isotherms were obeyed by the Schiff base in 1M HCl and 0.5M H₂SO₄ respectively. SEM analysis showed that DmChDa was adsorbed on the steel surface during corrosion inhibition. The variation of metal dissolution with temperature was also examined using gravimetric study.

Despite its well-reported application in a few welding processes, the use of reinforcing powders in weld joints to improve weld integrity has not garnered ample research attention for Gas Metal Arc Welding (GMAW) process. In this study, the adoption of Titanium alloy powders as metallic reinforcement for mild steel butt welds was investigated. By adopting Taguchi’s L4 orthogonal array, process optimisation for titanium-reinforced mild steel butt welds were first carried out. In the second phase of welding, the optimum parameters were used to create and compare two sets of weldments; one set was reinforced with titanium alloy powder and the other set left unreinforced. It was observed that in the Weld Metal (WM) region, the titanium-reinforced samples had higher micro-hardness values than their unreinforced counterparts with an average of 285.62 HV and 211.6 HV respectively. However, there was no substantial improvement in the ultimate tensile strength of the mild steel butt welds due to titanium powder reinforcements. Interestingly, the formation of acicular ferrite microstructure was more prevalent in the titanium-reinforced weldments and this was attributed to the presence of titanium inclusions in the weld metal. This prevalence of acicular ferrite suggests improved toughness properties in the weld joint region. While the higher hardness values in the Weld Metal of the reinforced sample indicates improved wear resistance.

The corrosion inhibition efficiencies of two novel Schiff bases, namely (E)-3-[thiophen-2-ylmethyleneamino]benzoic acid (T2YMABA) and (E)-4-(5-[(2-phenylhydrazono) methyl]thiophen-2-yl)benzoic acid (PHMT2YBA) on mild steel (MS) in 1.0M HCl solution has been investigated and compared using electrochemical impedance spectroscopy and potentiodynamic polarization analysis. The Schiff bases exhibited very good corrosion inhibitions on mild steel in 1.0M HCl medium and the inhibition efficiency increased with the increase in concentration of the inhibitor. Polarization studies revealed that T2YMABA acted as a mixed type inhibitor whereas PHMT2YBA molecules acted as anodic inhibitor.