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Growing Science » Authors » Masumeh Gilanizadeh

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Sort articles by: 📖 Volume | 📅 Date | ⭐ Most Rates | 👁️ Most Views | 🚀 Rising Stars | 📊 Citations (Scopus) | 🔥 Hot Papers
1.

Microwave-promoted three-component Hantzsch synthesis of acridinediones under green conditions Pages 71-78 Right click to download the paper Download PDF

Authors: Behzad Zeynizadeh, Masumeh Gilanizadeh

doi 10.5267/j.ccl.2019.8.001 Crossmark

🔑 Keywords: Acridinediones, Arylaldehydes, Dimedone, Hantzsch synthesis, Microwave Irradiation

Abstract:
In this study, a green and practical approach towards Hantzsch dihydropyridine synthesis of acridine-1,8-diones is introduced. Via the mentioned protocol, the one-pot condensation reaction of structurally diverse aromatic aldehydes, dimedone and NH4OAc was promoted by microwave radiation at solvent and catalyst-free conditions. Consequently, acridinedione products were produced in 81‒97% yields within 3‒8 min. The current protocol represents the prominent advantages in terms of the using a simple synthetic procedure, short reaction times, mild reaction conditions, high yield of the products as well as omission of hazardous and cost-effective organic solvents/reagents.

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Journal: CCL | Year: 2020 | Volume: 9 | Issue: 2 | Views: 2276

 
2.

Magnetically recoverable CuFe2O4 nanoparticles as an efficient heterogeneous catalyst for green formylation of alcohols Pages 121-130 Right click to download the paper Download PDF

Authors: Behzad Zeynizadeh, Elahe Gholamiyan, Masumeh Gilanizadeh

doi 10.5267/j.ccl.2018.11.001 Crossmark

🔑 Keywords: Alcohols CuFe2O4 Formylation Nanoparticles Super paramagnetic

Abstract:
In this article, magnetically nanoparticles (MNPs) of CuFe2O4 were prepared and characterized using Fourier transform infrared spectroscopy, scanning electron microscopy, X-ray diffraction and transmission electron microscopy techniques. Super paramagnetic CuFe2O4 was used as an efficient catalyst for green formylation of structurally diverse alcohols to the corresponding formyl esters using formic acid as a solvent (60-70 °C). All reactions were carried out successfully within 1-120 min to afford the products in 76-96 % yields. Reusibility of CuFe2O4 MNPs was examined 5 times without significant loss of its catalytic activity.
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Journal: CCL | Year: 2018 | Volume: 7 | Issue: 4 | Views: 2046

 
3.

4Å molecular sieves catalyzed ring-opening of epoxides to 1,2-diacetates with acetic anhydride Pages 153-158 Right click to download the paper Download PDF

Authors: Masumeh Gilanizadeh, Behzad Zeynizadeh

doi 10.5267/j.ccl.2015.6.002 Crossmark

🔑 Keywords: 1-2-Diacetate, Acetic anhydride, Epoxide, Molecular sieves, Ring-opening

Abstract:
This study was aimed at highly stereoselective ring-opening of epoxides with acetic anhydride in the presence of molecular sieves 4Å as an efficient reagent. Yields of the 1,2-diacetates are uniformly good to excellent and the reagent may be recycled without the requirement for purification. High yields, short reaction times, ease of preparation and simple work-up procedure (filtration) are advantages of this method.
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Journal: CCL | Year: 2015 | Volume: 4 | Issue: 4 | Views: 3038

 

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