How to cite this paper
El-Ossaily, Y., Alanazi, N., Althobaiti, I., Altaleb, H., Al-Muailkel, N., El-Sayed, M., Hussein, M., Ahmed, I., Alanazi, M., Fawzy, A., Abdel-Raheem, S & Tolba, M. (2024). Multicomponent approach to the synthesis and spectral characterization of some 3,5-pyrazolididione derivatives and evaluation as anti-inflammatory agents.Current Chemistry Letters, 13(1), 127-140.
Refrences
(1) Tundo P., Anastas P., Black D. S., Breen J., Collins T. J., Memoli S., Miyamoto J., Polyakoff M., and Tumas, W. (2000) Synthetic pathways and processes in green chemistry. Introductory overview. Pure Appl. Chem., 72 (7) 1207-1228.
(2) Alfonsi K., Colberg J., Dunn P. J., Fevig T., Jennings S., Johnson T. A., ... and Stefaniak M. (2008) Green chemistry tools to influence a medicinal chemistry and research chemistry based organisation. Green Chem., 10 (1) 31-36.
(3) Roughley S. D., and Jordan A. M. (2011) The medicinal chemist’s toolbox: an analysis of reactions used in the pursuit of drug candidates. J. Med. Chem., 54 (10) 3451-3479.
(4) Parikh N., Roy S. R., Seth K., Kumar A., and Chakraborti A. K. (2016) ‘On-water’multicomponent reaction for the diastereoselective synthesis of functionalized tetrahydropyridines and mechanistic insight. Synthesis, 48 (04) 547-556.
(5) Jadhavar P. S., Dhameliya T. M., Vaja M. D., Kumar D., Sridevi J. P., Yogeeswari P., ... and Chakraborti A. K. (2016) Synthesis, biological evaluation and structure–activity relationship of 2-styrylquinazolones as anti-tubercular agents. Bioorg. Med. Chem. Lett., 26 (11) 2663-2669.
(6) Kumar D., Jadhavar P. S., Nautiyal M., Sharma H., Meena P. K., Adane L., ... and Chakraborti A. K. (2015) Convenient synthesis of 2, 3-disubstituted quinazolin-4 (3 H)-ones and 2-styryl-3-substituted quinazolin-4 (3 H)-ones: Applications towards the synthesis of drugs. RSC Adv., 5 (39) 30819-30825.
(7) Kumar D., Kumar A., Qadri M. M., Ansari M. I., Gautam A., and Chakraborti A. K. (2015) In (OTf) 3-catalyzed synthesis of 2-styryl quinolines: scope and limitations of metal Lewis acids for tandem Friedländer annulation–Knoevenagel condensation. RSC Adv., 5 (4) 2920-2927.
(8) Kumar D., Sonawane M., Pujala B., Jain V. K., Bhagat S., and Chakraborti A. K. (2013) Supported protic acid-catalyzed synthesis of 2, 3-disubstituted thiazolidin-4-ones: enhancement of the catalytic potential of protic acid by adsorption on solid supports. Green Chem., 15 (10) 2872-2884.
(9) Kumar D., Kommi D. N., Bollineni N., Patel A. R., and Chakraborti A. K. (2012) Catalytic procedures for multicomponent synthesis of imidazoles: selectivity control during the competitive formation of tri-and tetrasubstituted imidazoles. Green Chem., 14 (7) 2038-2049.
(10) Khatik G. L., Kumar R., and Chakraborti A. K. (2006) Catalyst-free conjugated addition of thiols to α, β-unsaturated carbonyl compounds in water. Org. Lett., 8 (11) 2433-2436.
(11) Chankeshwara S. V., and Chakraborti A. K. (2006) Catalyst-free chemoselective N-tert-butyloxycarbonylation of amines in water. Org. Lett., 8 (15) 3259-3262.
(12) Chakraborti A. K., Rudrawar S., Jadhav K. B., Kaur G., and Chankeshwara S. V. (2007) “On water” organic synthesis: a highly efficient and clean synthesis of 2-aryl/heteroaryl/styryl benzothiazoles and 2-alkyl/aryl alkyl benzothiazolines. Green Chem., 9 (12) 1335-1340.
(13) Sharma G., Kumar R., and Chakraborti A. K. (2008) ‘On water’synthesis of 2,4-diaryl-2,3-dihydro-1,5-benzothiazepines catalysed by sodium dodecyl sulfate (SDS). Tetrahedron Lett., 49 (27) 4269-4271.
(14) RahaáRoy S. (2011) Surfactant mediated oxygen reuptake in water for green aerobic oxidation: mass-spectrometric determination of discrete intermediates to correlate oxygen uptake with oxidation efficiency. Chem. Commun., 47 (6) 1797-1799.
(15) Kommi D. N., Kumar D., Bansal R., Chebolu R., and Chakraborti A. K. (2012) “All-water” chemistry of tandem N-alkylation–reduction–condensation for synthesis of N-arylmethyl-2-substituted benzimidazoles. Green Chem., 14 (12) 3329-3335.
(16) Kommi D. N., Jadhavar P. S., Kumar D., and Chakraborti A. K. (2013) “All-water” one-pot diverse synthesis of 1, 2-disubstituted benzimidazoles: hydrogen bond driven ‘synergistic electrophile–nucleophile dual activation’by water. Green Chem., 15 (3) 798-810.
(17) Kommi D. N., Kumar D., and Chakraborti A. K. (2013) “All water chemistry” for a concise total synthesis of the novel class anti-anginal drug (RS),(R), and (S)-ranolazine. Green Chem., 15 (3) 756-767.
(18) Kumar D., Seth K., Kommi D. N., Bhagat S., and Chakraborti A. K. (2013) Surfactant micelles as microreactors for the synthesis of quinoxalines in water: scope and limitations of surfactant catalysis. RSC Adv., 3 (35) 15157-15168.
(19) Tanwar B., Purohit P., Raju B. N., Kumar D., Kommi D. N., and Chakraborti A. K. (2015) An “all-water” strategy for regiocontrolled synthesis of 2-aryl quinoxalines. RSC Adv., 5 (16) 11873-11883.
(20) Dhameliya T. M., Chourasiya S. S., Mishra E., Jadhavar P. S., Bharatam P. V., and Chakraborti A. K. (2017) Rationalization of benzazole-2-carboxylate versus benzazine-3-one/benzazine-2, 3-dione selectivity switch during cyclocondensation of 2-aminothiophenols/phenols/anilines with 1, 2-biselectrophiles in aqueous medium. J. Org. Chem., 82 (19) 10077-10091.
(21) Lee C. S., Allwine D. A., Barbachyn M. R., Grega K. C., Dolak L. A., Ford C. W., ... and Genin M. J. (2001) Carbon–carbon-linked (pyrazolylphenyl) oxazolidinones with antibacterial activity against multiple drug resistant gram-positive and fastidious gram-negative bacteria. Bioorg. Med. Chem., 9 (12) 3243-3253.
(22) Sridhar R., Perumal P. T., Etti S., Shanmugam G., Ponnuswamy M. N., Prabavathy V. R., and Mathivanan N. (2004) Design, synthesis and anti-microbial activity of 1H-pyrazole carboxylates. Bioorg. Med. Chem. Lett., 14 (24) 6035-6040.
(23) Ismail Z. H., Abdel-Gawad S. M., Abdel-Aziem A., and Ghorab M. M. (2003) Synthesis of some new biologically active sulfur compounds containing pyrazolo [3,4-d] pyrimidine moiety. Phosphorus. Sulfur. Silicon Relat. Elem., 178 (8) 1795-1805.
(24) Mamolo M. G., Falagiani V., Zampieri D., Vio L., and Banfi E. (2001) Synthesis and antimycobacterial activity of [5-(pyridin-2-yl)-1, 3, 4-thiadiazol-2-ylthio] acetic acid arylidene-hydrazide derivatives. Farm., 56 (8) 587-592.
(25) Hassan S. Y. (2013) Synthesis, antibacterial and antifungal activity of some new pyrazoline and pyrazole derivatives. Molecules, 18 (3) 2683-2711.
(26) Barnes B. J., Eakin A. E., Izydore R. A., and Hall I. H. (2000) Selective Inhibition of Human Molt-4 Leukemia Type II Inosine 5 ‘-Monophosphate Dehydrogenase by the 1,5-Diazabicyclo [3.1.0] hexane-2,4-diones. Biochemistry, 39 (45) 13641-13650.
(27) Dilek Altıntop M., Ozdemir A., Ilgın S., and Atli O. (2014) Synthesis and biological evaluation of new pyrazole-based thiazolyl hydrazone derivatives as potential anticancer agents. Lett. Drug Des. Discov., 11 (7) 833-839.
(28) Baraldi P. G., Pavani M. G., del Carmen Nunez M., Brigidi P., Vitali B., Gambari R., and Romagnoli R. (2002) Antimicrobial and antitumor activity of N-heteroimmine-1, 2, 3-dithiazoles and their transformation in triazolo-, imidazo-, and pyrazolopirimidines. Bioorg. Med. Chem., 10 (2) 449-456.
(29) Ochi T., Yamane-Sugiyama A., Ohkubo Y., Sakane K., and Tanaka H. (2001) The anti-inflammatory effect of FR188582, a highly selective inhibitor of cyclooxygenase-2, with an ulcerogenic sparing effect in rats. Jpn. J. Pharmacol., 85 (2) 175-182.
(30) Abdel-Aziz M., Abuo-Rahma G. E. D. A., and Hassan A. A. (2009) Synthesis of novel pyrazole derivatives and evaluation of their antidepressant and anticonvulsant activities. Eur. J. Med. Chem., 44 (9) 3480-3487.
(31) Pyo S. G. (2014) Characterization and Formation of Selectively Deposited Solar Electrode Using Electroless Plating Process. In Electrochemical Society Meeting Abstracts ecee2014 (No. 3, pp. 427-427). The Electrochemical Society, Inc.
(32) Baraldi P. G., Bovero A., Fruttarolo F., Romagnoli R., Tabrizi M. A., Preti D., ... and Moorman A. R. (2003) New strategies for the synthesis of A3 adenosine receptor antagonists. Bioorg. Med. Chem., 11 (19) 4161-4169.
(33) El-Sabbagh O. I., Baraka M. M., Ibrahim S. M., Pannecouque C., Andrei G., Snoeck R., ... and Rashad A. A. (2009) Synthesis and antiviral activity of new pyrazole and thiazole derivatives. Eur. J. Med. Chem., 44 (9) 3746-3753.
(34) Sayed M., Kamal El‐Dean A. M., Ahmed M., and Hassanien R. (2018) Synthesis, Characterization, and Screening for Anti‐inflammatory and Antimicrobial Activity of Novel Indolyl Chalcone Derivatives. J. Heterocycl. Chem., 55 (5) 1166-1175.
(35) Tolba M. S., Abdul-Malik M. A., Kamal El-Dean A. M., Geies A. A., Radwan Sh. M., Zaki R. M., Sayed M., Mohamed S. K., and Abdel-Raheem Sh. A. A. (2022) An overview on synthesis and reactions of coumarin based compounds. Curr. Chem. Lett., 11 (1) 29-42.
(36) Tolba M. S., Kamal El-Dean A. M., Ahmed M., Hassanien R., Sayed M., Zaki R. M., Mohamed S. K., Zawam S. A., and Abdel-Raheem Sh. A. A. (2022) Synthesis, reactions, and applications of pyrimidine derivatives. Curr. Chem. Lett., 11 (1) 121-138.
(37) Tolba M. S., Sayed M., Abdel-Raheem Sh. A. A., Gaber T. A., Kamal El-Dean A. M., and Ahmed M. (2021) Synthesis and spectral characterization of some new thiazolopyrimidine derivatives. Curr. Chem. Lett., 10 (4) 471-478.
(38) El-Zohry M. F., Younes M. I., and Metwally S. A. (1984) Synthesis and some reactions of 3-methyl-2-pyrazolin-4, 5-dione. Synthesis (Stuttg), 11 972-974.
(39) Metwally S. A., Mahfouz R. M., Elossaily Y. A., Aref S. A., and Naffea Y. A. (2016) Interaction of tetracyanoethylene (TCE) with active methylene compounds: synthesis, reactions and spectral characterization of some novel 2-pyrazoline-5-one compounds. Computational studies on the synthesized molecules by DFT. Assiut Univ. J. Chem., 45 33-46.
(40) El‐Ossaily Y. A., Metwally S. A., Al‐Muailkel N. S., Fawzy A., Ali H. M., and Naffea Y. A. (2020) Green synthetic investigation and spectral characterization of some spiro pyrazolidine‐based heterocycles with potential biological activity. J. Heterocycl. Chem., 57 (4) 1729-1736.
(41) Drück U., and Littke W. (1980) The structures of two rubazoic acid derivatives. Acta Crystallogr. Sect. B Struct. Crystallogr. Cryst. Chem., 36 (12) 3002-3007.
(42) Kirschke K., Hübner P., Lutze G., Gründemann E., and Ramm M. (1994) Ringtransformationen von 1‐Oxa‐5, 6‐diazaspiro [2.4] hept‐6‐en‐4‐onen zu 4,5‐Dihydro‐4‐hydroxy‐1H‐pyrazol‐4‐carbonsäure‐Derivaten. Liebigs Ann. Der Chemie., 1994 (2) 159-165.
(43) Metwally S. A. M., Mohamed T. A., Moustafa O. S., and El-Ossaily Y. A. (2011) Novel synthesis of highly functionalized pyrazolone systems via rearrangement of 5-phenyl-1-oxa-5,6-diazaspiro [2.4] heptane-4,7-diones. Chem. Heterocycl. Compd., 46 1344-1353.
(44) Younis O., Al-Hossainy A. F., Sayed M., El-dean A. M. K., and Tolba M. S. (2022) Synthesis and intriguing single-component white-light emission from oxadiazole or thiadiazole integrated with coumarin luminescent core. J. Photochem. Photobiol. A Chem., 431 113992.
(45) Mohamed S. K., El Bakri Y., Abdul D. A., Ahmad S., Albayati M. R., Lai C. H., ... and Tolba M. S. (2022) Synthesis, crystal structure, and a molecular modeling approach to identify effective antiviral hydrazide derivative against the main protease of SARS-CoV-2. J. Mol. Struct., 1265 133391.
(46) Siddekha A., Nizam A., and Pasha M. A. (2011) An efficient and simple approach for the synthesis of pyranopyrazoles using imidazole (catalytic) in aqueous medium, and the vibrational spectroscopic studies on 6-amino-4-(4′-methoxyphenyl)-5-cyano-3-methyl-1-phenyl-1,4-dihydropyrano[2,3-c] pyrazole using density functional theory. Spectrochim. Acta Part A Mol. Biomol. Spectrosc., 81 (1) 431-440.
(47) Kalla R. M. N., and Kim I. (2019) Highly efficient synthesis of pyrazolylphosphonate derivatives in biocompatible deep eutectic solvent. Mol. Catal., 473 110396.
(48) Martina K., Tagliapietra S., Veselov V. V., and Cravotto G. (2019) Green protocols in heterocycle syntheses via 1, 3-dipolar cycloadditions. Front. Chem., 7 95.
(49) Dekhici M., Plihon S., Bar N., Villemin D., Elsiblani H., and Cheikh N. (2019) Aerobic Copper Catalytic Oxidation of Methylene and Arylidenebisnaphthols: A Green and Efficient Synthesis of Spironaphthalenones. ChemistrySelect, 4 (2) 705-708.
(50) Shultz M. J., and Vu T. H. (2015) Hydrogen bonding between water and tetrahydrofuran relevant to clathrate formation. J. Phys. Chem. B., 119 (29) 9167-9172.
(51) Carvalho J. F., Silva M. M. C., and e Melo M. L. S. (2009) Highly efficient epoxidation of unsaturated steroids using magnesium bis (monoperoxyphthalate) hexahydrate. Tetrahedron, 65 (14) 2773-2781.
(52) Hamed M. M., Sayed M., Abdel-Mohsen S. A., Saddik A. A., Ibrahim O. A., El-Dean A. M. K., and Tolba M. S. (2023) Synthesis, biological evaluation, and molecular docking studies of novel diclofenac derivatives as antibacterial agents. J. Mol. Struct., 1273 134371.
(53) Almutlaq N., Elshanawany M. M., Sayed M., Younis O., Ahmed M., Wachtveitl J., ... and Abozeed A. A. (2023) Synthesis, structural, TD-DFT, and optical characteristics of indole derivatives. Curr. Appl. Phys., 45 86-98.
(54) Hussein E. M., Ahmed S. A., Guesmi N. E., and Khairou K. S. (2017) 1,3-Dipolar cycloaddition approach to novel dispiro [pyrazolidine-4,3′-pyrrolizidine-2′,3″-indoline]-2″,3,5-triones. J. Chem. Res., 41 (6) 346-351.
(55) Kamal R., Kumar R., Kumar V., and Bhardwaj V. (2019) Synthetic Utilization of α, β‐Chalcone Dibromide In Heterocyclic Chemistry and Stereoselective Debromination. ChemistrySelect, 4 (39) 11578-11603.
(56) Hsieh C. Y., Ko P. W., Chang Y. J., Kapoor M., Liang Y. C., Chu H. L., ... and Hsu M. H. (2019) Design and synthesis of benzimidazole-chalcone derivatives as potential anticancer agents. Molecules, 24 (18) 3259.
(57) Zimmerman H. E., Singer L., and Thyagarajan B. S. (1959) Overlap control of carbanionoid reactions. I. stereoselectivity in alkaline epoxidation. J. Am. Chem. Soc., 81 (1) 108-116.
(58) Singleton D. A., Merrigan S. R., Liu J., and Houk K. N. (1997) Experimental geometry of the epoxidation transition state. J. Am. Chem. Soc., 119 (14) 3385-3386.
(59) Tsumaki T. (1931) 3, 5-DIKETOPYRAZOLIDINE DERIVATIVES. I. Bull. Chem. Soc. Jpn., 6 (1) 1-8.
(60) Van Alphen J. (1924) The Action of Ketenes on Hydrazine Derivatives. Recl. Des Trav. Chim. Des Pays-Bas., 43 (12) 823-866.
(61) Bosso C., Marsura A., and Luu-Duc C. (1985) Mass spectra of 1,2,4-trisubstituted 5-functionalized 2-imidazolines. Org. Mass Spectrom., 20 (3) 263-264.
(62) Mustafa A., Sammour A., Kira M., Hilmy M. K., Anwar M., and Nakhla S. N. (1965) Beiträge zur Chemie der 3,5‐Pyrazolidindione. Arch. Pharm. (Weinheim)., 298 (8) 516-532.
(63) Kiran K., Sarasija M., Ananda Rao B., Namratha V., Ashok D., and Srinivasa Rao A. (2019) Design, synthesis, and biological activity of new bis-1,2,3-triazole derivatives bearing thiophene-chalcone moiety. Russ. J. Gen. Chem., 89 1859-1866.
(64) Metwally S. A., Mohamed T. A., Moustafa O. S., and El-Ossaily Y. A. (2007) Reactions of 4-alkylidene (arylidene)-1-phenylpyrazolidine-3,5-dione. Chem. Heterocycl. Compd., 43 1131-1137.
(65) Drar A. M., Abdel-Raheem Sh. A. A., Moustafa A. H., and Hussein B. R. M. (2023) Studying the toxicity and structure-activity relationships of some synthesized polyfunctionalized pyrimidine compounds as potential insecticides. Curr. Chem. Lett., 12 (3) 499-508.
(66) Abdel-Raheem Sh. A. A., Drar A. M., Hussein B. R. M., and Moustafa A. H. (2023) Some oxoimidazolidine and cyanoguanidine compounds: Toxicological efficacy and structure-activity relationships studies. Curr. Chem. Lett., 12 (4) 695–704.
(67) Abdel-Raheem Sh. A. A., Kamal El-Dean A. M., Hassanien R., El-Sayed M. E. A., and Abd-Ella A. A. (2021) Synthesis and characterization of some distyryl-derivatives for agricultural uses. Eur. Chem. Bull., 10 (1) 35-38.
(68) Kamal El-Dean A. M., Abd-Ella A. A., Hassanien R., El-Sayed M. E. A., Zaki R. M., and Abdel-Raheem Sh. A. A. (2019) Chemical design and toxicity evaluation of new pyrimidothienotetrahydroisoquinolines as potential insecticidal agents. Toxicol. Rep., 6 (2019) 100-104.
(69) Abdel-Raheem Sh. A. A., Kamal El-Dean A. M., Zaki R. M., Hassanien R., El-Sayed M. E. A., Sayed M., and Abd-Ella A. A. (2021) Synthesis and toxicological studies on distyryl-substituted heterocyclic insecticides. Eur. Chem. Bull., 10 (4) 225-229.
(70) Abdel-Raheem Sh. A. A., Kamal El-Dean A. M., Abdul-Malik M. A., Marae I. S., Bakhite E. A., Hassanien R., El-Sayed M. E. A., Zaki R. M., Tolba M. S., Sayed A. S. A., and Abd-Ella A. A. (2022) Facile synthesis and pesticidal activity of substituted heterocyclic pyridine compounds. Rev. Roum. Chem., 67 (4-5) 305-309.
(71) Ahmed A. A., Mohamed S. K., and Abdel-Raheem Sh. A. A. (2022) Assessment of the technological quality characters and chemical composition for some Egyptian Faba bean germplasm. Curr. Chem. Lett., 11 (4) 359-370.
(72) Tolba M. S., Sayed M., Kamal El-Dean A. M., Hassanien R., Abdel-Raheem Sh. A. A., and Ahmed M. (2021) Design, synthesis and antimicrobial screening of some new thienopyrimidines. Org. Commun., 14 (4) 334-345.
(73) Abdel-Raheem Sh. A. A., Kamal El-Dean A. M., Abdul-Malik M. A., Hassanien R., El-Sayed M. E. A., Abd-Ella A. A., Zawam S. A., and Tolba M. S. (2022) Synthesis of new distyrylpyridine analogues bearing amide substructure as effective insecticidal agents. Curr. Chem. Lett., 11 (1) 23-28.
(74) Abdel-Raheem Sh. A. A., Kamal El-Dean A. M., Abdul-Malik M. A., Abd-Ella A. A., Al-Taifi E. A., Hassanien R., El-Sayed M. E. A., Mohamed S. K., Zawam S. A., and Bakhite E. A. (2021) A concise review on some synthetic routes and applications of pyridine scaffold compounds. Curr. Chem. Lett., 10 (4) 337-362.
(75) Abdelhafeez I. A., El-Tohamy S. A., Abdul-Malik M. A., Abdel-Raheem Sh. A. A., and El-Dars F. M. S. (2022) A review on green remediation techniques for hydrocarbons and heavy metals contaminated soil. Curr. Chem. Lett., 11 (1) 43-62.
(76) Abdelhamid A. A., Elsaghier A. M. M., Aref S. A., Gad M. A., Ahmed N. A., and Abdel-Raheem Sh. A. A. (2021) Preparation and biological activity evaluation of some benzoylthiourea and benzoylurea compounds. Curr. Chem. Lett., 10 (4) 371-376.
(77) Elhady O. M., Mansour E. S., Elwassimy M. M., Zawam S. A., Drar A. M., and Abdel-Raheem Sh. A. A. (2022) Selective synthesis, characterization, and toxicological activity screening of some furan compounds as pesticidal agents. Curr. Chem. Lett., 11 (3) 285-290.
(78) Kaid M., Ali A. E., Shamsan A. Q. S., Salem W. M., Younes S. M., Abdel-Raheem Sh. A. A., and Abdul-Malik M. A. (2022) Efficiency of maturation oxidation ponds as a post-treatment technique of wastewater. Curr. Chem. Lett., 11 (4) 415-422.
(79) Mohamed S. K., Mague J. T., Akkurt M., Alfayomy A. M., Abou Seri S. M., Abdel-Raheem Sh. A. A., and Abdul-Malik M. A. (2022) Crystal structure and Hirshfeld surface analysis of ethyl (3E)-5-(4-chlorophenyl)-3-{[(4-chlorophenyl)formamido]imino}-7-methyl-2H,3H,5H-[1,3]thiazolo[3,2-a]pyrimidine-6-carboxylate. Acta Cryst., 78 (8) 846-850.
(80) El Bakri Y., Mohamed S. K., Saravanan K., Ahmad S., Mahmoud A. A., Abdel-Raheem Sh. A. A., ElSayed W. M., Mague J. T., and Said S. G. (2023) 1,4,9,9-tetramethyloctahydro-4,7-(epoxymethano)azulen-5(1H)-one, a natural product as a potential inhibitor of COVID-19: Extraction, crystal structure, and virtual screening approach. J. King Saud Univ. Sci., 35 (4) 102628.
(81) Abd-Ella A. A., Metwally S. A., Abdul-Malik M. A., El-Ossaily Y. A., AbdElrazek F. M., Aref S. A., Naffea Y. A., and Abdel-Raheem Sh. A. A. (2022) A review on recent advances for the synthesis of bioactive pyrazolinone and pyrazolidinedione derivatives. Curr. Chem. Lett., 11 (2) 157-172.
(82) Gad M. A., Aref S. A., Abdelhamid A. A., Elwassimy M. M., and Abdel-Raheem Sh. A. A. (2021) Biologically active organic compounds as insect growth regulators (IGRs): introduction, mode of action, and some synthetic methods. Curr. Chem. Lett., 10 (4) 393-412.
(83) Ibrahim S. M., Abdelkhalek A. S., Abdel-Raheem Sh. A. A., Freah N. E., El Hady N. H., Aidia N. K., Tawfeq N. A., Gomaa N. I., Fouad N. M., Salem H. A., Ibrahim H. M., and Sebaiy M. M. (2024) An overview on 2-indolinone derivatives as anticancer agents. Curr. Chem. Lett., Accepted Manuscript (DOI: 10.5267/j.ccl.2023.6.005).
(84) Abdel-Raheem Sh. A. A., Kamal El-Dean A. M., Hassanien R., El-Sayed M. E. A., Sayed M., and Abd-Ella A. A. (2021) Synthesis and spectral characterization of selective pyridine compounds as bioactive agents. Curr. Chem. Lett., 10 (3) 255-260.
(85) Fouad M. R., Shamsan A. Q. S., and Abdel-Raheem Sh. A. A. (2023) Toxicity of atrazine and metribuzin herbicides on earthworms (Aporrectodea caliginosa) by filter paper contact and soil mixing techniques. Curr. Chem. Lett., 12 (1) 185–192.
(86) Shamsan A. Q. S., Fouad M. R., Yacoob W. A. R. M., Abdul-Malik M. A., and Abdel-Raheem Sh. A. A. (2023) Performance of a variety of treatment processes to purify wastewater in the food industry. Curr. Chem. Lett., 12 (2) 431–438.
(87) Bakhite E. A., Abd-Ella A. A., El-Sayed M. E. A., and Abdel-Raheem Sh. A. A. (2014) Pyridine derivatives as insecticides. Part 1: Synthesis and toxicity of some pyridine derivatives against Cowpea Aphid, Aphis craccivora Koch (Homoptera: Aphididae). J. Agric. Food Chem., 62 (41) 9982–9986.
(88) Bakhite E. A., Abd-Ella A. A., El-Sayed M. E. A., and Abdel-Raheem Sh. A. A. (2017) Pyridine derivatives as insecticides. Part 2: Synthesis of some piperidinium and morpholiniumcyanopyridinethiolates and their Insecticidal Activity. J. Saud. Chem. Soc., 21 (1) 95–104.
(89) Kamal El-Dean A. M., Abd-Ella A. A., Hassanien R., El-Sayed M. E. A., and Abdel-Raheem Sh. A. A. (2019) Design, Synthesis, Characterization, and Insecticidal Bioefficacy Screening of Some New Pyridine Derivatives. ACS Omega, 4 (5) 8406-8412.
(90) Al-Taifi E. A., Abdel-Raheem Sh. A. A., and Bakhite E. A. (2016) Some reactions of 3-cyano-4-(p-methoxyphenyl)-5-oxo-5,6,7,8-tetrahydroquinoline-2(1H)-thione; Synthesis of new tetrahydroquinolines and tetrahydrothieno[2,3-b]quinolines. Assiut University Journal of Chemistry (AUJC), 45 (1) 24-32.
(91) Abdel-Raheem Sh. A. A., Kamal El-Dean A. M., Hassanien R., El-Sayed M. E. A., and Abd-Ella A. A. (2020) Synthesis and biological activity of 2-((3-Cyano-4,6-distyrylpyridin-2-yl)thio)acetamide and its cyclized form. Alger. j. biosciences, 01 (02) 046-050.
(92) Kula K., Łapczuk A., Sadowski M., Kras J., Zawadzińska K., Demchuk O. M., Gaurav G. K., Wróblewska A., and Jasiński R. (2022) On the Question of the Formation of Nitro-Functionalized 2,4-Pyrazole Analogs on the Basis of Nitrylimine Molecular Systems and 3,3,3-Trichloro-1-Nitroprop-1-Ene. Molecules, 27 (23) 8409.
(93) Fryźlewicz A., Kącka-Zych A., Demchuk O. M., Mirosław B., Woliński P., and Jasiński R. (2021) Green synthesis of nitrocyclopropane-type precursors of inhibitors for the maturation of fruits and vegetables via domino reactions of diazoalkanes with 2-nitroprop-1-ene. J. Clean. Prod., 292 126079.
(94) Kula K., Kącka-Zych A., Łapczuk-Krygier A., Wzorek Z., Nowak A. K., and Jasiński R. (2021) Experimental and theoretical mechanistic study on the thermal decomposition of 3,3-diphenyl-4-(trichloromethyl)-5-nitropyrazoline. Molecules, 26 (5) 1364.
(95) Sadowski M., Utnicka J., Wójtowicz A., and Kula K. (2023) The global and local Reactivity of C,N-diarylnitryle imines in [3+2] cycloaddition processes with trans-β-nitrostyrene according to Molecular Electron Density Theory: A computational study. Curr. Chem. Lett., 12 (2) 421-430.
(96) Kula K., and Zawadzińska K. (2021) Local nucleophile-electrophile interactions in [3+2] cycloaddition reactions between benzonitrile N-oxide and selected conjugated nitroalkenes in the light of MEDT computational study. Curr. Chem. Lett., 10 (1) 9-16.
(97) Domingo L. R., Kula K., Rios-Gutierrez M., and Jasinski R. (2021) Understanding the participation of fluorinated azomethine ylides in carbenoid-type [3+2] cycloaddition reactions with ynal systems: A molecular electron density theory study. J. Org. Chem., 86 (18) 12644-12653.
(98) Kula K., and Sadowski M. (2023) Regio-and stereoselectivity of [3+2] cycloaddition reactions between (Z)-1-(anthracen-9-yl)-N-methyl nitrone and analogs of trans-β-nitrostyrene on the basis of MEDT computational study. Chem. Heterocycl. Compd., 59 (3) 138–144.
(99) Kula K., Nagatsky R., Sadowski M., Siumka Y., and Demchuk O. M. (2023) Arylcyanomethylenequinone Oximes: An Overview of Synthesis, Chemical Transformations, and Biological Activity. Molecules, 28 (13) 5229.
(100) Zawadzińska K., Ríos-Gutiérrez M., Kula K., Woliński P., Mirosław B., Krawczyk T., and Jasiński R. (2021) The participation of 3,3,3-trichloro-1-nitroprop-1-ene in the [3+2] cycloaddition reaction with selected nitrile N-oxides in the light of the experimental and MEDT quantum chemical study. Molecules, 26 (22) 6774.
(101) Kula K., Dobosz J., Jasiński R., Kącka-Zych A., Łapczuk-Krygier A., Mirosław B., and Demchuk O. M. (2020) [3+2] Cycloaddition of diaryldiazomethanes with (E)-3,3,3-trichloro-1-nitroprop-1-ene: An experimental, theoretical and structural study. J. Mol. Struct., 1203 127473.
(102) Zawadzińska K., Gadocha Z., Pabian K., Wróblewska A., Wielgus E., and Jasiński R. (2022) The First Examples of [3+2] Cycloadditions with the Participation of (E)-3,3,3-tribromo-1-nitroprop-1-ene. Materials, 15 (21) 7584.
(103) Boguszewska-Czubara A., Kula K., Wnorowski A., Biernasiuk A., Popiołek Ł., Miodowski D., Demchuk O. M., and Jasiński R. (2019) Novel functionalized β-nitrostyrenes: Promising candidates for new antibacterial drugs. Saudi Pharm. J., 27 (4) 593-601.
(104) Boguszewska-Czubara A., Lapczuk-Krygier A., Rykala K., Biernasiuk A., Wnorowski A., Popiolek L., Maziarka A., Hordyjewska A., and Jasiński R. (2016) Novel synthesis scheme and in vitro antimicrobial evaluation of a panel of (E)-2-aryl-1-cyano-1-nitroethenes. J. Enzyme Inhib. Med. Chem., 31 (6) 900-907.
(105) Zawadzińska K., Gaurav G. K., and Jasiński R. (2022) Preparation of conjugated nitroalkenes: short review. Sci. Rad., 1 69-83.
(106) Woliński P., Kącka-Zych A., Mirosław B., Wielgus E., Olszewska A., and Jasiński R. (2022) Green, one-pot synthesis of 1,2-oxazine-type herbicides via non-catalyzed Hetero Diels-Alder reactions comprising (2E)-3-aryl-2-nitroprop-2-enenitriles. J. Clean. Prod., 356 131878.
(107) Ríos-Gutiérrez M., Domingo L. R., and Jasiński R. (2023) Unveiling the high reactivity of experimental pseudodiradical azomethine ylides within molecular electron density theory. Phys. Chem. Chem. Phys., 25 (1) 314-325.
(2) Alfonsi K., Colberg J., Dunn P. J., Fevig T., Jennings S., Johnson T. A., ... and Stefaniak M. (2008) Green chemistry tools to influence a medicinal chemistry and research chemistry based organisation. Green Chem., 10 (1) 31-36.
(3) Roughley S. D., and Jordan A. M. (2011) The medicinal chemist’s toolbox: an analysis of reactions used in the pursuit of drug candidates. J. Med. Chem., 54 (10) 3451-3479.
(4) Parikh N., Roy S. R., Seth K., Kumar A., and Chakraborti A. K. (2016) ‘On-water’multicomponent reaction for the diastereoselective synthesis of functionalized tetrahydropyridines and mechanistic insight. Synthesis, 48 (04) 547-556.
(5) Jadhavar P. S., Dhameliya T. M., Vaja M. D., Kumar D., Sridevi J. P., Yogeeswari P., ... and Chakraborti A. K. (2016) Synthesis, biological evaluation and structure–activity relationship of 2-styrylquinazolones as anti-tubercular agents. Bioorg. Med. Chem. Lett., 26 (11) 2663-2669.
(6) Kumar D., Jadhavar P. S., Nautiyal M., Sharma H., Meena P. K., Adane L., ... and Chakraborti A. K. (2015) Convenient synthesis of 2, 3-disubstituted quinazolin-4 (3 H)-ones and 2-styryl-3-substituted quinazolin-4 (3 H)-ones: Applications towards the synthesis of drugs. RSC Adv., 5 (39) 30819-30825.
(7) Kumar D., Kumar A., Qadri M. M., Ansari M. I., Gautam A., and Chakraborti A. K. (2015) In (OTf) 3-catalyzed synthesis of 2-styryl quinolines: scope and limitations of metal Lewis acids for tandem Friedländer annulation–Knoevenagel condensation. RSC Adv., 5 (4) 2920-2927.
(8) Kumar D., Sonawane M., Pujala B., Jain V. K., Bhagat S., and Chakraborti A. K. (2013) Supported protic acid-catalyzed synthesis of 2, 3-disubstituted thiazolidin-4-ones: enhancement of the catalytic potential of protic acid by adsorption on solid supports. Green Chem., 15 (10) 2872-2884.
(9) Kumar D., Kommi D. N., Bollineni N., Patel A. R., and Chakraborti A. K. (2012) Catalytic procedures for multicomponent synthesis of imidazoles: selectivity control during the competitive formation of tri-and tetrasubstituted imidazoles. Green Chem., 14 (7) 2038-2049.
(10) Khatik G. L., Kumar R., and Chakraborti A. K. (2006) Catalyst-free conjugated addition of thiols to α, β-unsaturated carbonyl compounds in water. Org. Lett., 8 (11) 2433-2436.
(11) Chankeshwara S. V., and Chakraborti A. K. (2006) Catalyst-free chemoselective N-tert-butyloxycarbonylation of amines in water. Org. Lett., 8 (15) 3259-3262.
(12) Chakraborti A. K., Rudrawar S., Jadhav K. B., Kaur G., and Chankeshwara S. V. (2007) “On water” organic synthesis: a highly efficient and clean synthesis of 2-aryl/heteroaryl/styryl benzothiazoles and 2-alkyl/aryl alkyl benzothiazolines. Green Chem., 9 (12) 1335-1340.
(13) Sharma G., Kumar R., and Chakraborti A. K. (2008) ‘On water’synthesis of 2,4-diaryl-2,3-dihydro-1,5-benzothiazepines catalysed by sodium dodecyl sulfate (SDS). Tetrahedron Lett., 49 (27) 4269-4271.
(14) RahaáRoy S. (2011) Surfactant mediated oxygen reuptake in water for green aerobic oxidation: mass-spectrometric determination of discrete intermediates to correlate oxygen uptake with oxidation efficiency. Chem. Commun., 47 (6) 1797-1799.
(15) Kommi D. N., Kumar D., Bansal R., Chebolu R., and Chakraborti A. K. (2012) “All-water” chemistry of tandem N-alkylation–reduction–condensation for synthesis of N-arylmethyl-2-substituted benzimidazoles. Green Chem., 14 (12) 3329-3335.
(16) Kommi D. N., Jadhavar P. S., Kumar D., and Chakraborti A. K. (2013) “All-water” one-pot diverse synthesis of 1, 2-disubstituted benzimidazoles: hydrogen bond driven ‘synergistic electrophile–nucleophile dual activation’by water. Green Chem., 15 (3) 798-810.
(17) Kommi D. N., Kumar D., and Chakraborti A. K. (2013) “All water chemistry” for a concise total synthesis of the novel class anti-anginal drug (RS),(R), and (S)-ranolazine. Green Chem., 15 (3) 756-767.
(18) Kumar D., Seth K., Kommi D. N., Bhagat S., and Chakraborti A. K. (2013) Surfactant micelles as microreactors for the synthesis of quinoxalines in water: scope and limitations of surfactant catalysis. RSC Adv., 3 (35) 15157-15168.
(19) Tanwar B., Purohit P., Raju B. N., Kumar D., Kommi D. N., and Chakraborti A. K. (2015) An “all-water” strategy for regiocontrolled synthesis of 2-aryl quinoxalines. RSC Adv., 5 (16) 11873-11883.
(20) Dhameliya T. M., Chourasiya S. S., Mishra E., Jadhavar P. S., Bharatam P. V., and Chakraborti A. K. (2017) Rationalization of benzazole-2-carboxylate versus benzazine-3-one/benzazine-2, 3-dione selectivity switch during cyclocondensation of 2-aminothiophenols/phenols/anilines with 1, 2-biselectrophiles in aqueous medium. J. Org. Chem., 82 (19) 10077-10091.
(21) Lee C. S., Allwine D. A., Barbachyn M. R., Grega K. C., Dolak L. A., Ford C. W., ... and Genin M. J. (2001) Carbon–carbon-linked (pyrazolylphenyl) oxazolidinones with antibacterial activity against multiple drug resistant gram-positive and fastidious gram-negative bacteria. Bioorg. Med. Chem., 9 (12) 3243-3253.
(22) Sridhar R., Perumal P. T., Etti S., Shanmugam G., Ponnuswamy M. N., Prabavathy V. R., and Mathivanan N. (2004) Design, synthesis and anti-microbial activity of 1H-pyrazole carboxylates. Bioorg. Med. Chem. Lett., 14 (24) 6035-6040.
(23) Ismail Z. H., Abdel-Gawad S. M., Abdel-Aziem A., and Ghorab M. M. (2003) Synthesis of some new biologically active sulfur compounds containing pyrazolo [3,4-d] pyrimidine moiety. Phosphorus. Sulfur. Silicon Relat. Elem., 178 (8) 1795-1805.
(24) Mamolo M. G., Falagiani V., Zampieri D., Vio L., and Banfi E. (2001) Synthesis and antimycobacterial activity of [5-(pyridin-2-yl)-1, 3, 4-thiadiazol-2-ylthio] acetic acid arylidene-hydrazide derivatives. Farm., 56 (8) 587-592.
(25) Hassan S. Y. (2013) Synthesis, antibacterial and antifungal activity of some new pyrazoline and pyrazole derivatives. Molecules, 18 (3) 2683-2711.
(26) Barnes B. J., Eakin A. E., Izydore R. A., and Hall I. H. (2000) Selective Inhibition of Human Molt-4 Leukemia Type II Inosine 5 ‘-Monophosphate Dehydrogenase by the 1,5-Diazabicyclo [3.1.0] hexane-2,4-diones. Biochemistry, 39 (45) 13641-13650.
(27) Dilek Altıntop M., Ozdemir A., Ilgın S., and Atli O. (2014) Synthesis and biological evaluation of new pyrazole-based thiazolyl hydrazone derivatives as potential anticancer agents. Lett. Drug Des. Discov., 11 (7) 833-839.
(28) Baraldi P. G., Pavani M. G., del Carmen Nunez M., Brigidi P., Vitali B., Gambari R., and Romagnoli R. (2002) Antimicrobial and antitumor activity of N-heteroimmine-1, 2, 3-dithiazoles and their transformation in triazolo-, imidazo-, and pyrazolopirimidines. Bioorg. Med. Chem., 10 (2) 449-456.
(29) Ochi T., Yamane-Sugiyama A., Ohkubo Y., Sakane K., and Tanaka H. (2001) The anti-inflammatory effect of FR188582, a highly selective inhibitor of cyclooxygenase-2, with an ulcerogenic sparing effect in rats. Jpn. J. Pharmacol., 85 (2) 175-182.
(30) Abdel-Aziz M., Abuo-Rahma G. E. D. A., and Hassan A. A. (2009) Synthesis of novel pyrazole derivatives and evaluation of their antidepressant and anticonvulsant activities. Eur. J. Med. Chem., 44 (9) 3480-3487.
(31) Pyo S. G. (2014) Characterization and Formation of Selectively Deposited Solar Electrode Using Electroless Plating Process. In Electrochemical Society Meeting Abstracts ecee2014 (No. 3, pp. 427-427). The Electrochemical Society, Inc.
(32) Baraldi P. G., Bovero A., Fruttarolo F., Romagnoli R., Tabrizi M. A., Preti D., ... and Moorman A. R. (2003) New strategies for the synthesis of A3 adenosine receptor antagonists. Bioorg. Med. Chem., 11 (19) 4161-4169.
(33) El-Sabbagh O. I., Baraka M. M., Ibrahim S. M., Pannecouque C., Andrei G., Snoeck R., ... and Rashad A. A. (2009) Synthesis and antiviral activity of new pyrazole and thiazole derivatives. Eur. J. Med. Chem., 44 (9) 3746-3753.
(34) Sayed M., Kamal El‐Dean A. M., Ahmed M., and Hassanien R. (2018) Synthesis, Characterization, and Screening for Anti‐inflammatory and Antimicrobial Activity of Novel Indolyl Chalcone Derivatives. J. Heterocycl. Chem., 55 (5) 1166-1175.
(35) Tolba M. S., Abdul-Malik M. A., Kamal El-Dean A. M., Geies A. A., Radwan Sh. M., Zaki R. M., Sayed M., Mohamed S. K., and Abdel-Raheem Sh. A. A. (2022) An overview on synthesis and reactions of coumarin based compounds. Curr. Chem. Lett., 11 (1) 29-42.
(36) Tolba M. S., Kamal El-Dean A. M., Ahmed M., Hassanien R., Sayed M., Zaki R. M., Mohamed S. K., Zawam S. A., and Abdel-Raheem Sh. A. A. (2022) Synthesis, reactions, and applications of pyrimidine derivatives. Curr. Chem. Lett., 11 (1) 121-138.
(37) Tolba M. S., Sayed M., Abdel-Raheem Sh. A. A., Gaber T. A., Kamal El-Dean A. M., and Ahmed M. (2021) Synthesis and spectral characterization of some new thiazolopyrimidine derivatives. Curr. Chem. Lett., 10 (4) 471-478.
(38) El-Zohry M. F., Younes M. I., and Metwally S. A. (1984) Synthesis and some reactions of 3-methyl-2-pyrazolin-4, 5-dione. Synthesis (Stuttg), 11 972-974.
(39) Metwally S. A., Mahfouz R. M., Elossaily Y. A., Aref S. A., and Naffea Y. A. (2016) Interaction of tetracyanoethylene (TCE) with active methylene compounds: synthesis, reactions and spectral characterization of some novel 2-pyrazoline-5-one compounds. Computational studies on the synthesized molecules by DFT. Assiut Univ. J. Chem., 45 33-46.
(40) El‐Ossaily Y. A., Metwally S. A., Al‐Muailkel N. S., Fawzy A., Ali H. M., and Naffea Y. A. (2020) Green synthetic investigation and spectral characterization of some spiro pyrazolidine‐based heterocycles with potential biological activity. J. Heterocycl. Chem., 57 (4) 1729-1736.
(41) Drück U., and Littke W. (1980) The structures of two rubazoic acid derivatives. Acta Crystallogr. Sect. B Struct. Crystallogr. Cryst. Chem., 36 (12) 3002-3007.
(42) Kirschke K., Hübner P., Lutze G., Gründemann E., and Ramm M. (1994) Ringtransformationen von 1‐Oxa‐5, 6‐diazaspiro [2.4] hept‐6‐en‐4‐onen zu 4,5‐Dihydro‐4‐hydroxy‐1H‐pyrazol‐4‐carbonsäure‐Derivaten. Liebigs Ann. Der Chemie., 1994 (2) 159-165.
(43) Metwally S. A. M., Mohamed T. A., Moustafa O. S., and El-Ossaily Y. A. (2011) Novel synthesis of highly functionalized pyrazolone systems via rearrangement of 5-phenyl-1-oxa-5,6-diazaspiro [2.4] heptane-4,7-diones. Chem. Heterocycl. Compd., 46 1344-1353.
(44) Younis O., Al-Hossainy A. F., Sayed M., El-dean A. M. K., and Tolba M. S. (2022) Synthesis and intriguing single-component white-light emission from oxadiazole or thiadiazole integrated with coumarin luminescent core. J. Photochem. Photobiol. A Chem., 431 113992.
(45) Mohamed S. K., El Bakri Y., Abdul D. A., Ahmad S., Albayati M. R., Lai C. H., ... and Tolba M. S. (2022) Synthesis, crystal structure, and a molecular modeling approach to identify effective antiviral hydrazide derivative against the main protease of SARS-CoV-2. J. Mol. Struct., 1265 133391.
(46) Siddekha A., Nizam A., and Pasha M. A. (2011) An efficient and simple approach for the synthesis of pyranopyrazoles using imidazole (catalytic) in aqueous medium, and the vibrational spectroscopic studies on 6-amino-4-(4′-methoxyphenyl)-5-cyano-3-methyl-1-phenyl-1,4-dihydropyrano[2,3-c] pyrazole using density functional theory. Spectrochim. Acta Part A Mol. Biomol. Spectrosc., 81 (1) 431-440.
(47) Kalla R. M. N., and Kim I. (2019) Highly efficient synthesis of pyrazolylphosphonate derivatives in biocompatible deep eutectic solvent. Mol. Catal., 473 110396.
(48) Martina K., Tagliapietra S., Veselov V. V., and Cravotto G. (2019) Green protocols in heterocycle syntheses via 1, 3-dipolar cycloadditions. Front. Chem., 7 95.
(49) Dekhici M., Plihon S., Bar N., Villemin D., Elsiblani H., and Cheikh N. (2019) Aerobic Copper Catalytic Oxidation of Methylene and Arylidenebisnaphthols: A Green and Efficient Synthesis of Spironaphthalenones. ChemistrySelect, 4 (2) 705-708.
(50) Shultz M. J., and Vu T. H. (2015) Hydrogen bonding between water and tetrahydrofuran relevant to clathrate formation. J. Phys. Chem. B., 119 (29) 9167-9172.
(51) Carvalho J. F., Silva M. M. C., and e Melo M. L. S. (2009) Highly efficient epoxidation of unsaturated steroids using magnesium bis (monoperoxyphthalate) hexahydrate. Tetrahedron, 65 (14) 2773-2781.
(52) Hamed M. M., Sayed M., Abdel-Mohsen S. A., Saddik A. A., Ibrahim O. A., El-Dean A. M. K., and Tolba M. S. (2023) Synthesis, biological evaluation, and molecular docking studies of novel diclofenac derivatives as antibacterial agents. J. Mol. Struct., 1273 134371.
(53) Almutlaq N., Elshanawany M. M., Sayed M., Younis O., Ahmed M., Wachtveitl J., ... and Abozeed A. A. (2023) Synthesis, structural, TD-DFT, and optical characteristics of indole derivatives. Curr. Appl. Phys., 45 86-98.
(54) Hussein E. M., Ahmed S. A., Guesmi N. E., and Khairou K. S. (2017) 1,3-Dipolar cycloaddition approach to novel dispiro [pyrazolidine-4,3′-pyrrolizidine-2′,3″-indoline]-2″,3,5-triones. J. Chem. Res., 41 (6) 346-351.
(55) Kamal R., Kumar R., Kumar V., and Bhardwaj V. (2019) Synthetic Utilization of α, β‐Chalcone Dibromide In Heterocyclic Chemistry and Stereoselective Debromination. ChemistrySelect, 4 (39) 11578-11603.
(56) Hsieh C. Y., Ko P. W., Chang Y. J., Kapoor M., Liang Y. C., Chu H. L., ... and Hsu M. H. (2019) Design and synthesis of benzimidazole-chalcone derivatives as potential anticancer agents. Molecules, 24 (18) 3259.
(57) Zimmerman H. E., Singer L., and Thyagarajan B. S. (1959) Overlap control of carbanionoid reactions. I. stereoselectivity in alkaline epoxidation. J. Am. Chem. Soc., 81 (1) 108-116.
(58) Singleton D. A., Merrigan S. R., Liu J., and Houk K. N. (1997) Experimental geometry of the epoxidation transition state. J. Am. Chem. Soc., 119 (14) 3385-3386.
(59) Tsumaki T. (1931) 3, 5-DIKETOPYRAZOLIDINE DERIVATIVES. I. Bull. Chem. Soc. Jpn., 6 (1) 1-8.
(60) Van Alphen J. (1924) The Action of Ketenes on Hydrazine Derivatives. Recl. Des Trav. Chim. Des Pays-Bas., 43 (12) 823-866.
(61) Bosso C., Marsura A., and Luu-Duc C. (1985) Mass spectra of 1,2,4-trisubstituted 5-functionalized 2-imidazolines. Org. Mass Spectrom., 20 (3) 263-264.
(62) Mustafa A., Sammour A., Kira M., Hilmy M. K., Anwar M., and Nakhla S. N. (1965) Beiträge zur Chemie der 3,5‐Pyrazolidindione. Arch. Pharm. (Weinheim)., 298 (8) 516-532.
(63) Kiran K., Sarasija M., Ananda Rao B., Namratha V., Ashok D., and Srinivasa Rao A. (2019) Design, synthesis, and biological activity of new bis-1,2,3-triazole derivatives bearing thiophene-chalcone moiety. Russ. J. Gen. Chem., 89 1859-1866.
(64) Metwally S. A., Mohamed T. A., Moustafa O. S., and El-Ossaily Y. A. (2007) Reactions of 4-alkylidene (arylidene)-1-phenylpyrazolidine-3,5-dione. Chem. Heterocycl. Compd., 43 1131-1137.
(65) Drar A. M., Abdel-Raheem Sh. A. A., Moustafa A. H., and Hussein B. R. M. (2023) Studying the toxicity and structure-activity relationships of some synthesized polyfunctionalized pyrimidine compounds as potential insecticides. Curr. Chem. Lett., 12 (3) 499-508.
(66) Abdel-Raheem Sh. A. A., Drar A. M., Hussein B. R. M., and Moustafa A. H. (2023) Some oxoimidazolidine and cyanoguanidine compounds: Toxicological efficacy and structure-activity relationships studies. Curr. Chem. Lett., 12 (4) 695–704.
(67) Abdel-Raheem Sh. A. A., Kamal El-Dean A. M., Hassanien R., El-Sayed M. E. A., and Abd-Ella A. A. (2021) Synthesis and characterization of some distyryl-derivatives for agricultural uses. Eur. Chem. Bull., 10 (1) 35-38.
(68) Kamal El-Dean A. M., Abd-Ella A. A., Hassanien R., El-Sayed M. E. A., Zaki R. M., and Abdel-Raheem Sh. A. A. (2019) Chemical design and toxicity evaluation of new pyrimidothienotetrahydroisoquinolines as potential insecticidal agents. Toxicol. Rep., 6 (2019) 100-104.
(69) Abdel-Raheem Sh. A. A., Kamal El-Dean A. M., Zaki R. M., Hassanien R., El-Sayed M. E. A., Sayed M., and Abd-Ella A. A. (2021) Synthesis and toxicological studies on distyryl-substituted heterocyclic insecticides. Eur. Chem. Bull., 10 (4) 225-229.
(70) Abdel-Raheem Sh. A. A., Kamal El-Dean A. M., Abdul-Malik M. A., Marae I. S., Bakhite E. A., Hassanien R., El-Sayed M. E. A., Zaki R. M., Tolba M. S., Sayed A. S. A., and Abd-Ella A. A. (2022) Facile synthesis and pesticidal activity of substituted heterocyclic pyridine compounds. Rev. Roum. Chem., 67 (4-5) 305-309.
(71) Ahmed A. A., Mohamed S. K., and Abdel-Raheem Sh. A. A. (2022) Assessment of the technological quality characters and chemical composition for some Egyptian Faba bean germplasm. Curr. Chem. Lett., 11 (4) 359-370.
(72) Tolba M. S., Sayed M., Kamal El-Dean A. M., Hassanien R., Abdel-Raheem Sh. A. A., and Ahmed M. (2021) Design, synthesis and antimicrobial screening of some new thienopyrimidines. Org. Commun., 14 (4) 334-345.
(73) Abdel-Raheem Sh. A. A., Kamal El-Dean A. M., Abdul-Malik M. A., Hassanien R., El-Sayed M. E. A., Abd-Ella A. A., Zawam S. A., and Tolba M. S. (2022) Synthesis of new distyrylpyridine analogues bearing amide substructure as effective insecticidal agents. Curr. Chem. Lett., 11 (1) 23-28.
(74) Abdel-Raheem Sh. A. A., Kamal El-Dean A. M., Abdul-Malik M. A., Abd-Ella A. A., Al-Taifi E. A., Hassanien R., El-Sayed M. E. A., Mohamed S. K., Zawam S. A., and Bakhite E. A. (2021) A concise review on some synthetic routes and applications of pyridine scaffold compounds. Curr. Chem. Lett., 10 (4) 337-362.
(75) Abdelhafeez I. A., El-Tohamy S. A., Abdul-Malik M. A., Abdel-Raheem Sh. A. A., and El-Dars F. M. S. (2022) A review on green remediation techniques for hydrocarbons and heavy metals contaminated soil. Curr. Chem. Lett., 11 (1) 43-62.
(76) Abdelhamid A. A., Elsaghier A. M. M., Aref S. A., Gad M. A., Ahmed N. A., and Abdel-Raheem Sh. A. A. (2021) Preparation and biological activity evaluation of some benzoylthiourea and benzoylurea compounds. Curr. Chem. Lett., 10 (4) 371-376.
(77) Elhady O. M., Mansour E. S., Elwassimy M. M., Zawam S. A., Drar A. M., and Abdel-Raheem Sh. A. A. (2022) Selective synthesis, characterization, and toxicological activity screening of some furan compounds as pesticidal agents. Curr. Chem. Lett., 11 (3) 285-290.
(78) Kaid M., Ali A. E., Shamsan A. Q. S., Salem W. M., Younes S. M., Abdel-Raheem Sh. A. A., and Abdul-Malik M. A. (2022) Efficiency of maturation oxidation ponds as a post-treatment technique of wastewater. Curr. Chem. Lett., 11 (4) 415-422.
(79) Mohamed S. K., Mague J. T., Akkurt M., Alfayomy A. M., Abou Seri S. M., Abdel-Raheem Sh. A. A., and Abdul-Malik M. A. (2022) Crystal structure and Hirshfeld surface analysis of ethyl (3E)-5-(4-chlorophenyl)-3-{[(4-chlorophenyl)formamido]imino}-7-methyl-2H,3H,5H-[1,3]thiazolo[3,2-a]pyrimidine-6-carboxylate. Acta Cryst., 78 (8) 846-850.
(80) El Bakri Y., Mohamed S. K., Saravanan K., Ahmad S., Mahmoud A. A., Abdel-Raheem Sh. A. A., ElSayed W. M., Mague J. T., and Said S. G. (2023) 1,4,9,9-tetramethyloctahydro-4,7-(epoxymethano)azulen-5(1H)-one, a natural product as a potential inhibitor of COVID-19: Extraction, crystal structure, and virtual screening approach. J. King Saud Univ. Sci., 35 (4) 102628.
(81) Abd-Ella A. A., Metwally S. A., Abdul-Malik M. A., El-Ossaily Y. A., AbdElrazek F. M., Aref S. A., Naffea Y. A., and Abdel-Raheem Sh. A. A. (2022) A review on recent advances for the synthesis of bioactive pyrazolinone and pyrazolidinedione derivatives. Curr. Chem. Lett., 11 (2) 157-172.
(82) Gad M. A., Aref S. A., Abdelhamid A. A., Elwassimy M. M., and Abdel-Raheem Sh. A. A. (2021) Biologically active organic compounds as insect growth regulators (IGRs): introduction, mode of action, and some synthetic methods. Curr. Chem. Lett., 10 (4) 393-412.
(83) Ibrahim S. M., Abdelkhalek A. S., Abdel-Raheem Sh. A. A., Freah N. E., El Hady N. H., Aidia N. K., Tawfeq N. A., Gomaa N. I., Fouad N. M., Salem H. A., Ibrahim H. M., and Sebaiy M. M. (2024) An overview on 2-indolinone derivatives as anticancer agents. Curr. Chem. Lett., Accepted Manuscript (DOI: 10.5267/j.ccl.2023.6.005).
(84) Abdel-Raheem Sh. A. A., Kamal El-Dean A. M., Hassanien R., El-Sayed M. E. A., Sayed M., and Abd-Ella A. A. (2021) Synthesis and spectral characterization of selective pyridine compounds as bioactive agents. Curr. Chem. Lett., 10 (3) 255-260.
(85) Fouad M. R., Shamsan A. Q. S., and Abdel-Raheem Sh. A. A. (2023) Toxicity of atrazine and metribuzin herbicides on earthworms (Aporrectodea caliginosa) by filter paper contact and soil mixing techniques. Curr. Chem. Lett., 12 (1) 185–192.
(86) Shamsan A. Q. S., Fouad M. R., Yacoob W. A. R. M., Abdul-Malik M. A., and Abdel-Raheem Sh. A. A. (2023) Performance of a variety of treatment processes to purify wastewater in the food industry. Curr. Chem. Lett., 12 (2) 431–438.
(87) Bakhite E. A., Abd-Ella A. A., El-Sayed M. E. A., and Abdel-Raheem Sh. A. A. (2014) Pyridine derivatives as insecticides. Part 1: Synthesis and toxicity of some pyridine derivatives against Cowpea Aphid, Aphis craccivora Koch (Homoptera: Aphididae). J. Agric. Food Chem., 62 (41) 9982–9986.
(88) Bakhite E. A., Abd-Ella A. A., El-Sayed M. E. A., and Abdel-Raheem Sh. A. A. (2017) Pyridine derivatives as insecticides. Part 2: Synthesis of some piperidinium and morpholiniumcyanopyridinethiolates and their Insecticidal Activity. J. Saud. Chem. Soc., 21 (1) 95–104.
(89) Kamal El-Dean A. M., Abd-Ella A. A., Hassanien R., El-Sayed M. E. A., and Abdel-Raheem Sh. A. A. (2019) Design, Synthesis, Characterization, and Insecticidal Bioefficacy Screening of Some New Pyridine Derivatives. ACS Omega, 4 (5) 8406-8412.
(90) Al-Taifi E. A., Abdel-Raheem Sh. A. A., and Bakhite E. A. (2016) Some reactions of 3-cyano-4-(p-methoxyphenyl)-5-oxo-5,6,7,8-tetrahydroquinoline-2(1H)-thione; Synthesis of new tetrahydroquinolines and tetrahydrothieno[2,3-b]quinolines. Assiut University Journal of Chemistry (AUJC), 45 (1) 24-32.
(91) Abdel-Raheem Sh. A. A., Kamal El-Dean A. M., Hassanien R., El-Sayed M. E. A., and Abd-Ella A. A. (2020) Synthesis and biological activity of 2-((3-Cyano-4,6-distyrylpyridin-2-yl)thio)acetamide and its cyclized form. Alger. j. biosciences, 01 (02) 046-050.
(92) Kula K., Łapczuk A., Sadowski M., Kras J., Zawadzińska K., Demchuk O. M., Gaurav G. K., Wróblewska A., and Jasiński R. (2022) On the Question of the Formation of Nitro-Functionalized 2,4-Pyrazole Analogs on the Basis of Nitrylimine Molecular Systems and 3,3,3-Trichloro-1-Nitroprop-1-Ene. Molecules, 27 (23) 8409.
(93) Fryźlewicz A., Kącka-Zych A., Demchuk O. M., Mirosław B., Woliński P., and Jasiński R. (2021) Green synthesis of nitrocyclopropane-type precursors of inhibitors for the maturation of fruits and vegetables via domino reactions of diazoalkanes with 2-nitroprop-1-ene. J. Clean. Prod., 292 126079.
(94) Kula K., Kącka-Zych A., Łapczuk-Krygier A., Wzorek Z., Nowak A. K., and Jasiński R. (2021) Experimental and theoretical mechanistic study on the thermal decomposition of 3,3-diphenyl-4-(trichloromethyl)-5-nitropyrazoline. Molecules, 26 (5) 1364.
(95) Sadowski M., Utnicka J., Wójtowicz A., and Kula K. (2023) The global and local Reactivity of C,N-diarylnitryle imines in [3+2] cycloaddition processes with trans-β-nitrostyrene according to Molecular Electron Density Theory: A computational study. Curr. Chem. Lett., 12 (2) 421-430.
(96) Kula K., and Zawadzińska K. (2021) Local nucleophile-electrophile interactions in [3+2] cycloaddition reactions between benzonitrile N-oxide and selected conjugated nitroalkenes in the light of MEDT computational study. Curr. Chem. Lett., 10 (1) 9-16.
(97) Domingo L. R., Kula K., Rios-Gutierrez M., and Jasinski R. (2021) Understanding the participation of fluorinated azomethine ylides in carbenoid-type [3+2] cycloaddition reactions with ynal systems: A molecular electron density theory study. J. Org. Chem., 86 (18) 12644-12653.
(98) Kula K., and Sadowski M. (2023) Regio-and stereoselectivity of [3+2] cycloaddition reactions between (Z)-1-(anthracen-9-yl)-N-methyl nitrone and analogs of trans-β-nitrostyrene on the basis of MEDT computational study. Chem. Heterocycl. Compd., 59 (3) 138–144.
(99) Kula K., Nagatsky R., Sadowski M., Siumka Y., and Demchuk O. M. (2023) Arylcyanomethylenequinone Oximes: An Overview of Synthesis, Chemical Transformations, and Biological Activity. Molecules, 28 (13) 5229.
(100) Zawadzińska K., Ríos-Gutiérrez M., Kula K., Woliński P., Mirosław B., Krawczyk T., and Jasiński R. (2021) The participation of 3,3,3-trichloro-1-nitroprop-1-ene in the [3+2] cycloaddition reaction with selected nitrile N-oxides in the light of the experimental and MEDT quantum chemical study. Molecules, 26 (22) 6774.
(101) Kula K., Dobosz J., Jasiński R., Kącka-Zych A., Łapczuk-Krygier A., Mirosław B., and Demchuk O. M. (2020) [3+2] Cycloaddition of diaryldiazomethanes with (E)-3,3,3-trichloro-1-nitroprop-1-ene: An experimental, theoretical and structural study. J. Mol. Struct., 1203 127473.
(102) Zawadzińska K., Gadocha Z., Pabian K., Wróblewska A., Wielgus E., and Jasiński R. (2022) The First Examples of [3+2] Cycloadditions with the Participation of (E)-3,3,3-tribromo-1-nitroprop-1-ene. Materials, 15 (21) 7584.
(103) Boguszewska-Czubara A., Kula K., Wnorowski A., Biernasiuk A., Popiołek Ł., Miodowski D., Demchuk O. M., and Jasiński R. (2019) Novel functionalized β-nitrostyrenes: Promising candidates for new antibacterial drugs. Saudi Pharm. J., 27 (4) 593-601.
(104) Boguszewska-Czubara A., Lapczuk-Krygier A., Rykala K., Biernasiuk A., Wnorowski A., Popiolek L., Maziarka A., Hordyjewska A., and Jasiński R. (2016) Novel synthesis scheme and in vitro antimicrobial evaluation of a panel of (E)-2-aryl-1-cyano-1-nitroethenes. J. Enzyme Inhib. Med. Chem., 31 (6) 900-907.
(105) Zawadzińska K., Gaurav G. K., and Jasiński R. (2022) Preparation of conjugated nitroalkenes: short review. Sci. Rad., 1 69-83.
(106) Woliński P., Kącka-Zych A., Mirosław B., Wielgus E., Olszewska A., and Jasiński R. (2022) Green, one-pot synthesis of 1,2-oxazine-type herbicides via non-catalyzed Hetero Diels-Alder reactions comprising (2E)-3-aryl-2-nitroprop-2-enenitriles. J. Clean. Prod., 356 131878.
(107) Ríos-Gutiérrez M., Domingo L. R., and Jasiński R. (2023) Unveiling the high reactivity of experimental pseudodiradical azomethine ylides within molecular electron density theory. Phys. Chem. Chem. Phys., 25 (1) 314-325.